Viewing services matching the following properties:
1H-NMR spectrum of sample dissolved in D2O or DMSO-d6 with heating up to 80 °C.
Equipment associated with this service:
The spark plasma sintering of such powders as carbides, carbonitrides, nitrides, oxides, and their composites.
Determination according to ISO 12091: 1995
Determination according to LVS EN 11357-6:2013 / LVS EN 728:2000
Folin-Denis or Folin-Ciocalteu method
Porosity (%) and pore size/volume distribution of solid samples. Intended for the materials such as catalysts, surgical implants, electrodes, concrete, ceramics and metallic compounds, pharmaceuticals, membranes, filters, etc.
Potentiometric titration in aqueous or non-aqueous media
The Carbon Coater is one of the most advanced sample coaters available for coating of non-conductive specimens prior to SEM X-ray analysis. Carbon is best used for EDS application.
Sputter coating for SEM is a process of applying an ultra-thin coating of electrically-conducting metal onto a non-conducting or poorly conducting specimen. Coating of samples is required to enable or improve the imaging of samples. Creation of a conductive layer of metal on the sample inhibits charging, reduces thermal damage and improves the secondary electron signal required for topographic examination in the SEM. The coating technique that should be used depends on the required resolution and application. Chromium sputtered surface has very fine grain size which is most useful for FESEM imaging. Gold target is excellent and most widely used target material for standard SEM coating. But it should be noted that grain size is visible at high magnifications. Platinum/Paladium is also adequate for FESEM imaging. Its grain size is similar to Pt.
Processing of SEM images, compositional measurements by SEM/EDS and obtained data interpretation. The major sections of the report are: introduction, sample preparation, experimental, results, discussion, conclusion, references and appendix.